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Beilstein J. Org. Chem. 2022, 18, 788–795, doi:10.3762/bjoc.18.79
Graphical Abstract
Scheme 1: Envisioned Minisci perfluoroalkylation facilitated by “dummy group” reagents 1a–c.
Scheme 2: Control experiments for the nucleophilic substitution of perfluoroalkylsulfinates 2 and halogenated...
Scheme 3: Left: isolated yields of synthesized perfluoroalkylating reagents: perfluorobutyl (1a), perfluorohe...
Scheme 4: Radical trapping experiment with 1,1-diphenylethylene (7) and 1b confirming the initially proposed ...
Scheme 5: Demonstrative scope for the perfluoroalkylation of aromatics. Isolated yields are shown in parenthe...
Beilstein J. Org. Chem. 2016, 12, 2636–2643, doi:10.3762/bjoc.12.260
Scheme 1: Design light-mediated arylation of THIQs.
Figure 1: Reaction scope. Reaction conditions: THIQs (0.10 mmol), arylboronic acid (0.30 mmol), TBHP (0.2 mmo...
Scheme 2: Evaluation of chiral ligands.
Scheme 3: Proposed reaction mechanism.
Beilstein J. Org. Chem. 2013, 9, 1388–1396, doi:10.3762/bjoc.9.155
Scheme 1: Sketch illustrating preparation of the Au@HS-CNC catalyst.
Figure 1: Au4f and S2p XPS spectra of the Au@HS-CNC (4.4 mol %) catalyst.
Figure 2: TEM pictures of the HS-NCC and Au@HS-CNC (4.4 mol %) catalyst (scale bar: 5 nm).
Figure 3: Thermogravimetric behavior of the Au@HS-CNC (4.4 mol %) catalyst (A) and CNC (B).
Figure 4: FT-IR spectra of CNC, HS-CNC, and Au@HS-CNC (4.4 mol %) catalyst.
Figure 5: Solid-state 13C NMR spectra of the CNC and Au@HS-CNC (4.4 mol %) catalyst.
Figure 6: Recycling test of Au@HS-CNC (4.4 mol %) catalyst for the three-component coupling of formaldehyde, ...